Search results for "lattice [perturbation theory]"

showing 10 items of 139 documents

NMR T1-Relaxation Measurements on Paramagnetic Organolanthanides: An Alternative Tool for Structure Determination in Solution

2005

1H NMR investigations were conducted on four paramagnetic organolanthanides, all bearing the tetraisopropylcyclopentadienyl ligand Cp4i (HC5iPr4) in order to verify whether or not interactions observed in the solid state are maintained in solution. In some cases variable-temperature experiments were necessary to enhance the resolution and determine the best conditions for the study. The 1D NMR spectrum could be interpreted in every case. Complementary 2D COSY experiments allowed the full attribution of the signals. T1 (1H) relaxation values were determined for all the paramagnetic complexes at the most suitable temperature, and compared with those of the diamagnetic KCp4i. The same tendency…

010405 organic chemistryChemistryLigandRelaxation (NMR)Analytical chemistrySpin–lattice relaxation[ CHIM.COOR ] Chemical Sciences/Coordination chemistryNuclear magnetic resonance spectroscopy010402 general chemistry01 natural sciences0104 chemical sciencesParamagnetic complexesInorganic Chemistrychemistry.chemical_compoundParamagnetismCrystallographyNMR spectroscopyOxidation stateLanthanidesProton NMR[CHIM.COOR]Chemical Sciences/Coordination chemistryMethyl groupSpin-lattice relaxation times
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High‐nuclearity mixed‐valence magnetic clusters : A general solution of the double exchange problem

1996

We report here a general solution of the double‐exchange problem in the high‐nuclearity mixed valence systems containing arbitrary number P of the electrons delocalized over the network of N (P<N) localized spins. The developed approach is based on the successive (chainlike) spin‐coupling scheme and takes full advantage from the quantum angular momentum theory. In the framework of this approach the closed‐form analytical expressions are deduced for the matrix elements of the double exchange interaction, two‐electron transfer, and three‐center interaction that can be referred to as the potential exchange transfer. For the arbitrary nuclearity mixed‐valence systems the matrix elements of all …

Angular momentumValence (chemistry)SpinsChemistryExchange interactionExchange InteractionsGeneral Physics and AstronomyElectron TransferQuantum numberLocalized StatesUNESCO::FÍSICA::Química físicaDelocalized electronMolecular ClustersQuantum mechanicsMixed−Valence CompoundsPhysical and Theoretical ChemistryMatrix ElementsSpin−Lattice Relaxation:FÍSICA::Química física [UNESCO]Exchange Interactions ; Molecular Clusters ; Matrix Elements ; Electron Transfer ; Localized States ; Spin−Lattice Relaxation ; Mixed−Valence CompoundsQuantumBasis set
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Reorientations and translations in a fragile glass-former: magnetic resonance studies of meta-fluoroaniline

1999

Abstract The rotational dynamics in supercooled liquid and glassy meta-fluoroaniline was studied using proton and fluorine spin-lattice relaxation times. It is shown that while proton relaxation is dominated by homonuclear relaxation, for fluorine heteronuclear relaxation prevails. The results could be well described using a distribution of correlation times. The mean correlation times show pronounced deviations from the simple Arrhenius law. In addition translational self-diffusion coefficients were measured for T>200 K using a static magnetic field gradient technique.

Arrhenius equationCondensed matter physicsProtonChemistryOrganic ChemistrySpin–lattice relaxationMagnetostaticsHomonuclear moleculeAnalytical ChemistryInorganic ChemistrySpin–spin relaxationsymbols.namesakeHeteronuclear moleculesymbolsRelaxation (physics)SpectroscopyJournal of Molecular Structure
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Iterative momentum relaxation for fast lattice-boltzmann simulations

1999

Lattice-Boltzmann simulations are often used for studying steady-state hydrodynamics. In these simulations, however, the complete time evolution starting from some initial condition is redundantly computed due to the transient nature of the scheme. In this article we present a refinement of body-force driven lattice-Boltzmann simulations that may reduce the simulation time significantly. This new technique is based on an iterative adjustment of the local body-force and is validated on a realistic test case, namely fluid flow in a static mixer reactor.

Body forceComputer sciencebusiness.industryTime evolutionLattice Boltzmann methodsRelaxation (iterative method)MechanicsComputational fluid dynamicsStatic mixerlaw.inventionMomentumlawFluid dynamicsInitial value problembusinessAlgorithm
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A Novel Radiotherapeutic Approach to Treat Bulky Metastases Even From Cutaneous Squamous Cell Carcinoma: Its Rationale and a Look at the Reliability …

2022

IntroductionMetastatic cutaneous squamous cell carcinoma (cSCC) is a very rare condition. The lack of definition of an oligometastatic subgroup means that there is no consensus for its treatment, unlike the mucosal head and neck counterpart. Like the latter, the cutaneous form is able to develop bulky tumor masses. When this happens, the classic care approach is just for palliative intent due to a likely unfavorable benefit–risk balance typical of aggressive treatments. Here we proposed a novel radiotherapy (RT) technique to treat bulky metastases from cSCC in the context of an overall limited tumor burden and tried to explain its clinical outcome by the currently available mathematical rad…

Cancer ResearchOncologycutaneous squamous cell carcinomatumor control probability (TCP)spatially fractionated radiation therapynormal tissue complication probability (NTCP)immunotherapylattice radiotherapybulky tumorsSettore FIS/07 - Fisica Applicata(Beni Culturali Ambientali Biol.e Medicin)metabolic tumor volume
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Finite-size scaling in a microcanonical ensemble

1988

The finite-size scaling technique is extended to a microcanonical ensemble. As an application, equilibrium magnetic properties of anL×L square lattice Ising model are computed using the microcanonical ensemble simulation technique of Creutz, and the results are analyzed using the microcanonical ensemble finite-size scaling. The computations were done on the multitransputer system of the Condensed Matter Theory Group at the University of Mainz.

Canonical ensembleStatistical ensemblePhysicsMicrocanonical ensembleThermodynamic betaIsothermal–isobaric ensembleCondensed Matter::Statistical MechanicsStatistical and Nonlinear PhysicsIsing modelSquare-lattice Ising modelStatistical mechanicsStatistical physicsMathematical PhysicsJournal of Statistical Physics
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Self-trapped exciton luminescence in crystalline α-quartz under two-photon laser excitation

2003

Abstract The luminescence of pure crystalline α-quartz is studied under pulsed ArF laser excitation. The luminescence parameters obtained correspond well with those of self-trapped excitons (STEs) in α-quartz, indicating that the excitation process is two-photon. The efficiency of two-photon excitation is of the same order of magnitude as the one-photon excitation of sodium salicylate. The STE luminescence decay kinetics and their temperature dependence under photoexcitation were recorded with higher accuracy than previously. Changes in the decay kinetics with temperature are explained by the splitting of the STE triplet state in zero magnetic field and are analyzed with the assumption of t…

ChemistryExcitonRelaxation (NMR)Spin–lattice relaxationPhysics::OpticsGeneral ChemistryCondensed Matter PhysicsPhotoexcitationCondensed Matter::Materials ScienceTwo-photon excitation microscopyPhysics::Atomic and Molecular ClustersMaterials ChemistryTriplet stateAtomic physicsLuminescenceExcitationSolid State Communications
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Low-temperature methyl group dynamics of hexamethylbenzene in crystalline and glassy matrices as studied by 2H NMR

1991

Abstract 2 H NMR spectra of hexamethylbenzene (HMB) in protonated crystalline and amorphous matrices at low temperatures are presented. All spectra reveal lineshape changes which can be attributed to methyl group tunnelling. Compared to neat HMB, a drastic increase of the tunnelling frequency is found for all systems. This indicates that the hindering potential originates predominantly from intermolecular forces. We studied the temperature dependence of these spectra and the spin-lattice relaxation in order to exclude a distribution of motional correlation times describing a thermally activated process. In addition, we find a distortion of the methyl tetrahedron.

ChemistryIntermolecular forceRelaxation (NMR)Spin–lattice relaxationGeneral Physics and AstronomyNuclear magnetic resonance spectroscopyAmorphous solidchemistry.chemical_compoundNuclear magnetic resonanceProton NMRHexamethylbenzenePhysical chemistryPhysical and Theoretical ChemistryMethyl groupChemical Physics Letters
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Site-Specific Information on Membrane Protein Folding by Electron Spin Echo Envelope Modulation Spectroscopy

2010

Compared to folding of soluble proteins, folding of membrane proteins is complicated by the fact that it requires an amphiphilic environment. Few existing techniques can provide structurally resolved information on folding kinetics. For the major plant light harvesting complex LHCII, it is demonstrated that changes in water accessibility of a particular amino acid residue can be followed during folding by measuring the hyperfine interaction of spin labels with deuterium nuclei of heavy water. The incorporation of residue 196 into the hydrophobic core of a detergent micelle was investigated. The technique provides a time constant that is similar to the one found with fluorescence spectroscop…

ChemistryPhi value analysisSite-directed spin labelinglaw.inventionFolding (chemistry)CrystallographylawLattice proteinBiophysicsGeneral Materials ScienceProtein foldingDownhill foldingPhysical and Theoretical ChemistryElectron paramagnetic resonanceSpin labelThe Journal of Physical Chemistry Letters
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Phase transition kinetics and reorientational dynamics of the plastic crystal meta-carborane studied by deuteron NMR

2002

Meta-carborane shows an orientationally disordered, orthorhombic phase which transforms into an ordered monoclinic phase near 170 K and into a quasi-isotropic cubic phase near 280 K. From deuteron magnetization measurements both transitions are found to exhibit a thermal hysteresis and slow transformation kinetics. Furthermore, solid-echo NMR spectra and spin-lattice relaxation times are reported. These results indicate that in the orthorhombic phase the meta-carborane molecules perform a strongly anisotropic motion which is characterized by a temperature dependent amplitude.

ChemistryRelaxation (NMR)Spin–lattice relaxationThermodynamicsCondensed Matter Physics530Electronic Optical and Magnetic MaterialsNMR spectra databaseMagnetizationCrystallographyCondensed Matter::Materials SciencePhase (matter)Materials ChemistryCeramics and CompositesOrthorhombic crystal systemCondensed Matter::Strongly Correlated ElectronsPlastic crystalMonoclinic crystal system
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